1,4,7,10,13,16,19,22,25,28,31,34,37,40,43,46-hexadecaoxacyclooctatetracontane

Base Information

Chemical Name:1,4,7,10,13,16,19,22,25,28,31,34,37,40,43,46-hexadecaoxacyclooctatetracontane
CAS No.:71092-61-0
Molecular Formula:C₃₂H₆₄O₁₆
Molecular Weight:704.851
Hs Code.:

Synonyms:48-Crown-16

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4,7,10,13,16,19,22,25,28,31,34,37,40,43,46-hexadecaoxacyclooctatetracontane

Chemical Property:

Vapor Pressure:0mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4,7,10,13,16,19,22,25,28,31,34,37,40,43,46-hexadecaoxacyclooctatetracontane

There total 4 articles about 1,4,7,10,13,16,19,22,25,28,31,34,37,40,43,46-hexadecaoxacyclooctatetracontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 112-60-7
Tetraethylene glycol

: 33089-37-1
24-crown-8

: 71092-61-0
48-Crown-16

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) 40 min, 2.) 67 deg C, 34 h;
DOI:10.1021/jo00087a040

Reference yield: 23.0%

: 112-60-7
Tetraethylene glycol

: 294-93-9,64491-37-8
(1,4,7,10-tetraoxacyclododecane)

: 33089-37-1
24-crown-8

: 71092-59-6
<36>crown-12

: 71092-61-0
48-Crown-16

Guidance literature:: With potassium hydroxide; p-toluenesulfonyl chloride; In 1,4-dioxane; at 65 ℃; Further byproducts given;
DOI:10.1016/S0040-4020(01)80080-6

Reference yield: 23.0%

: 112-60-7
Tetraethylene glycol

: 33089-37-1
24-crown-8

: 71092-63-2
<60>crown-20

: 71092-59-6
<36>crown-12

: 71092-61-0
48-Crown-16

Guidance literature:: With potassium hydroxide; p-toluenesulfonyl chloride; In 1,4-dioxane; at 65 ℃; Further byproducts given;
DOI:10.1016/S0040-4020(01)80080-6