1,3,6,9,12,15,18,21-Octaoxacyclotetracosane

Base Information

Chemical Name:1,3,6,9,12,15,18,21-Octaoxacyclotetracosane
CAS No.:33089-37-1
Molecular Formula:C16H32O8
Molecular Weight:352.425
Hs Code.:2932999099
DSSTox Substance ID:DTXSID80954714
Mol file:33089-37-1.mol

Synonyms:1,3,6,9,12,15,18,21-octaoxacyclotetracosane;BRN 1686140;EINECS 251-374-9;DTXSID80954714

Suppliers and Price of 1,3,6,9,12,15,18,21-Octaoxacyclotetracosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
24-Crown 8-Ether >95.0%(GC)
1g
$ 372.00

American Custom Chemicals Corporation
24-CROWN 8-ETHER 95.00%
1G
$ 872.70

AK Scientific
24-Crown 8-Ether
1g
$ 548.00

Total 15 raw suppliers

Chemical Property of 1,3,6,9,12,15,18,21-Octaoxacyclotetracosane

Chemical Property:

Vapor Pressure:2.18E-09mmHg at 25°C
Refractive Index:1.404
Boiling Point:497.6 °C at 760 mmHg
Flash Point:202.8 °C
PSA：73.84000
Density:0.995 g/cm³
LogP:0.13280
XLogP3:-0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:0
Exact Mass:352.20971797
Heavy Atom Count:24
Complexity:242

Purity/Quality:

98%,99%, ^*data from raw suppliers

24-Crown 8-Ether >95.0%(GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 20/21/22
Safety Statements: 36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOCCOCCOCCOCCOCCOCOC1

Technology Process of 1,3,6,9,12,15,18,21-Octaoxacyclotetracosane

There total 11 articles about 1,3,6,9,12,15,18,21-Octaoxacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 112-60-7
Tetraethylene glycol

: 33089-37-1
24-crown-8

: 71092-61-0
48-Crown-16

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) 40 min, 2.) 67 deg C, 34 h;
DOI:10.1021/jo00087a040

Reference yield: 39.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 112-60-7
Tetraethylene glycol

: 33089-37-1
24-crown-8

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 22 - 24 ℃; for 96h;
DOI:10.1080/00397919908085989

Reference yield: 23.0%

: 112-60-7
Tetraethylene glycol

: 294-93-9,64491-37-8
(1,4,7,10-tetraoxacyclododecane)

: 33089-37-1
24-crown-8

: 71092-59-6
<36>crown-12

: 71092-61-0
48-Crown-16

Guidance literature:: With potassium hydroxide; p-toluenesulfonyl chloride; In 1,4-dioxane; at 65 ℃; Further byproducts given;
DOI:10.1016/S0040-4020(01)80080-6