erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

Base Information

Chemical Name:erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether
CAS No.:120578-99-6
Molecular Formula:C₃₆H₄₂O₄
Molecular Weight:538.727
Hs Code.:

Synonyms:erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

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Chemical Property of erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

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Technology Process of erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

There total 7 articles about erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 6-hydroxy-5,6-bis(4-methoxyphenyl)octanoate

: 120578-99-6
erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 45.5 percent / H₂, perchloric acid / Pd/C / acetic acid / 2250.2 Torr

2: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

3: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

4: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

5: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

6: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

With lithium aluminium tetrahydride; perchloric acid; potassium tert-butylate; hydrogen; boron tribromide; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1021/jm00127a023

Reference yield:

: 100-39-0
benzyl bromide

: 120578-99-6
erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

2: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

3: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

4: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

With lithium aluminium tetrahydride; potassium tert-butylate; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; In tetrahydrofuran;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120578-99-6
erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl 2-hydroxyethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

2: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

3: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

4: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

With lithium aluminium tetrahydride; potassium tert-butylate; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; In tetrahydrofuran;
DOI:10.1021/jm00127a023