Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Base Information

Chemical Name:Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid
CAS No.:141020-18-0
Molecular Formula:C₄₆H₄₇NO₁₅
Molecular Weight:853.877
Hs Code.:

Synonyms:Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Suppliers and Price of Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

There total 9 articles about Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3601-36-3,6344-46-3
methyl 2,3,6-tri-O-benzoyl-α-D-galactopyranoside

: 141020-18-0
Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / pyridine / CH₂Cl₂ / 48 h / Ambient temperature

2: 94 percent / Bu3SnH, α,α'-azoisobutyronitrile / toluene / 4 h / Heating

3: 94 percent / iodotrimethylsilane / toluene / 3 h / Ambient temperature

4: 1.) Hg(CN)2, molecular sieves 4 Angstroem / 1.) dichloromethane, 1 h, 2.) 10 deg C, 5 h

5: 60 percent aq. acetic acid / 3 h / 40 °C

6: pyridine / 24 h

With pyridine; trimethylsilyl iodide; 4 A molecular sieve; azobisisobutyronitrile; tri-n-butyl-tin hydride; mercury(II) cyanide; acetic acid; In dichloromethane; toluene;

Reference yield:

: 19488-41-6
Methyl-2,3,6-tri-O-benzoyl-4-desoxy-α-D-xylo-hexopyranosid

: 141020-18-0
Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / iodotrimethylsilane / toluene / 3 h / Ambient temperature

2: 1.) Hg(CN)2, molecular sieves 4 Angstroem / 1.) dichloromethane, 1 h, 2.) 10 deg C, 5 h

3: 60 percent aq. acetic acid / 3 h / 40 °C

4: pyridine / 24 h

With pyridine; trimethylsilyl iodide; 4 A molecular sieve; mercury(II) cyanide; acetic acid; In toluene;

Reference yield:

: 141020-13-5
Methyl-2,3,6-tri-O-benzoyl-4-O-phenoxythiocarbonyl-α-D-galactopyranosid

: 141020-18-0
Benzyl-O-(2,3,6-tri-O-benzoyl-4-desoxy-β-D-xylo-hexopyranosyl)-(1->3)-2-acetamido-4,6-di-O-acetyl-2-desoxy-α-D-galactopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / Bu3SnH, α,α'-azoisobutyronitrile / toluene / 4 h / Heating

2: 94 percent / iodotrimethylsilane / toluene / 3 h / Ambient temperature

3: 1.) Hg(CN)2, molecular sieves 4 Angstroem / 1.) dichloromethane, 1 h, 2.) 10 deg C, 5 h

4: 60 percent aq. acetic acid / 3 h / 40 °C

5: pyridine / 24 h

With pyridine; trimethylsilyl iodide; 4 A molecular sieve; azobisisobutyronitrile; tri-n-butyl-tin hydride; mercury(II) cyanide; acetic acid; In toluene;