N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide

Base Information

• Chemical Name: N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide
• CAS No.: 335654-28-9
• Molecular Formula: C₆₈H₆₅NO₉
• Molecular Weight: 1040.27

Synonyms:N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide

Chemical Property of N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide

There total 3 articles about N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.1%

N-butylamine (109-73-9,85404-21-3) + 1,6,7,12-tetrakis(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid dianhydride (156028-30-7) → N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide (335654-28-9)

Guidance literature:

In toluene; for 1h; Inert atmosphere; Reflux;

DOI:10.1021/ol801668r

Reference yield: 24.0%

N,N'-dibutyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid bisimide (335654-34-7) → N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide (335654-28-9)

Guidance literature:

N,N'-dibutyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid bisimide; With potassium hydroxide; In water; isopropyl alcohol; for 3h; Reflux;

With hydrogenchloride; In water; isopropyl alcohol; at 20 - 90 ℃; for 1h;

DOI:10.1021/ol3029115

Reference yield:

N,N'-dibutyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid bisimide (335654-34-7) → 1,6,7,12-tetrakis(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid dianhydride (156028-30-7) + N-n-butyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4-dicarboxylate anhydride-9,10-dicarboxylate imide (335654-28-9)

Guidance literature:

With potassium hydroxide; water; In isopropyl alcohol; for 13h; Reflux;

DOI:10.1039/b719095f

upstream raw materials:

N,N'-dibutyl-1,6,7,12-tetra(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid bisimide

N-butylamine

1,6,7,12-tetrakis(4-tert-butylphenoxy)perylene-3,4:9,10-tetracarboxylic acid dianhydride

Downstream raw materials:

2-butyl-5,6,12,13-tetrakis-(4-tert-butyl-phenoxy)-9-(4-[2,2';6',2'']terpyridin-4'-yl-phenyl)-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

C₉₀H₁₀₀N₂O₈S₈

C₇₄H₇₀BF₂N₃O₇

C₁₀₆H₉₁N₅O₁₃

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