(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Base Information

Chemical Name:(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal
CAS No.:1335130-88-5
Molecular Formula:C₃₉H₄₅N₅O₉S₂
Molecular Weight:791.946
Hs Code.:

(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Synonyms:(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Chemical Property of (2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

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Technology Process of (2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

There total 6 articles about (2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1037070-06-6
(2S)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-pyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 1335130-79-4
(E)-3-(4-(3-azidopropoxy)-3-methoxyphenyl)-1-(4-hydroxyphenyl)prop-2-en-1-one

: 1335130-88-5
(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 1335130-73-8
4-(3-azidopropyloxy)-3-methoxybenzaldehyde

: 1335130-88-5
(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol; water / 12 h / 20 °C

1.2: pH 1

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 12 h / 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; potassium hydroxide; In methanol; water; tert-butyl alcohol; 1.1: Aldol condensation;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1335130-88-5
(2S)-N-{4-{(1-(3-(4-((E)-3-(4-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)propyl)-1H-1,2,3-triazol-4-yl)methoxy}-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyldithioacetal

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / Reflux

2.1: sodium azide / 6 h / 80 °C

3.1: potassium hydroxide / methanol; water / 12 h / 20 °C

3.2: pH 1

4.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 12 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Aldol condensation;
DOI:10.1016/j.ejmech.2011.05.050