C₃₃H₃₆N₂O₇S

Base Information

Chemical Name:C₃₃H₃₆N₂O₇S
CAS No.:1256489-09-4
Molecular Formula:C₃₃H₃₆N₂O₇S
Molecular Weight:604.724
Hs Code.:

C<sub>33</sub>H<sub>36</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₃₃H₃₆N₂O₇S

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Chemical Property of C₃₃H₃₆N₂O₇S

Chemical Property:

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Technology Process of C₃₃H₃₆N₂O₇S

There total 13 articles about C₃₃H₃₆N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256489-08-3
C₃₃H₃₄N₂O₇S

: 1256489-09-4
C₃₃H₃₆N₂O₇S

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 4h;

Reference yield:

: 52200-49-4
3-bromo-2-(phenylmethoxy)pyridine

: 1256489-09-4
C₃₃H₃₆N₂O₇S

Guidance literature:: Multi-step reaction with 4 steps

1: potassium acetate; bis(pinacol)diborane / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 26 h / 70 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; dichloromethane / 0.5 h / 100 °C / Sealed tube; Microwave Irradiation

3: potassium hydroxide / ethanol / 1.5 h / Reflux

4: sodium tetrahydroborate / ethanol / 4 h

With sodium tetrahydroborate; potassium acetate; sodium carbonate; bis(pinacol)diborane; potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;

Reference yield:

: 856898-35-6
methyl 2-bromo-5-[(methylsulfonyl)amino]benzoate

: 1256489-09-4
C₃₃H₃₆N₂O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / N,N-dimethyl-formamide / Inert atmosphere

1.2: 6 h / 75 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / -30 - 20 °C

3.1: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 70 °C

4.1: gold(III) chloride / trifluoroacetic acid / 0.75 h / 100 °C / Sealed tube; Microwave Irradiation

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; dichloromethane / 0.5 h / 100 °C / Sealed tube; Microwave Irradiation

6.1: potassium hydroxide / ethanol / 1.5 h / Reflux

7.1: sodium tetrahydroborate / ethanol / 4 h

With sodium tetrahydroborate; copper(l) iodide; tetrabutyl ammonium fluoride; sodium carbonate; triethylamine; potassium hydroxide; gold(III) chloride; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; trifluoroacetic acid;