methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate

Base Information

• Chemical Name: methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate
• CAS No.: 1160183-59-4
• Molecular Formula: C₃₀H₅₂O₁₅
• Molecular Weight: 652.734

Synonyms:methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate

Chemical Property of methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate

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Technology Process of methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate

There total 1 articles about methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

methyl-4-benzyloxy-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzoate → methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate (1160183-59-4)

Guidance literature:

With hydrogenchloride; palladium on activated charcoal; hydrogen; In ethanol; water; for 72h; under 37503.8 Torr; Autoclave;

DOI:10.1002/anie.200900143

Reference yield: 90.0%

methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate (1160183-59-4) + 2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate (1264015-76-0) → methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate (1264015-79-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 4h;

DOI:10.1039/c0cc02084b

Reference yield: 70.0%

2[-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl p-tosylate (906007-10-1) + methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate (1160183-59-4) → methyl-4-{2[-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzoate (1160183-60-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃;

DOI:10.1002/anie.200900143

Downstream raw materials:

methyl-4-{2[-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-benzoate

methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

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