2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Base Information

Chemical Name:2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate
CAS No.:1264015-76-0
Molecular Formula:C₂₄H₄₁NO₁₀S
Molecular Weight:535.656
Hs Code.:

Synonyms:2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Suppliers and Price of 2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

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Technology Process of 2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

There total 6 articles about 2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: tert-butyl tert-butyl (17-hydroxy-3,6,9,12,15-pentaoxaheptadecyl)carbamate

: 98-59-9
p-toluenesulfonyl chloride

: 1264015-76-0
2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 62.0%

: 331242-61-6
tert-butyl N-[2-[2-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethyl]carbamate

: 1264015-76-0
2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Guidance literature:: With triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c0cc02084b

Reference yield:

: 86770-69-6
17-azido-3,6,9,12,15-pentaoxaheptadecan-1-ol

: 1264015-76-0
2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 10% palladium on activated carbon; hydrogen / ethanol; water / 48 h / 7500.75 Torr / Autoclave

2.1: 1,4-dioxane / 3 h / 0 °C

2.2: 20 °C

3.1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

With 10% palladium on activated carbon; hydrogen; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1039/c0cc02084b