methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

Base Information

Chemical Name:methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate
CAS No.:1264015-79-3
Molecular Formula:C₄₇H₈₅NO₂₂
Molecular Weight:1016.19
Hs Code.:

methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

Synonyms:methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

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Chemical Property of methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

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Technology Process of methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

There total 4 articles about methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1160183-59-4
methyl-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-4-hydroxybenzoate

: 1264015-76-0
2-{2-[2-(2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy)ethoxy]ethoxy}ethyl p-tosylate

: 1264015-79-3
methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1039/c0cc02084b

Reference yield:

: 331242-61-6
tert-butyl N-[2-[2-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethyl]carbamate

: 1264015-79-3
methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

With potassium carbonate; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0cc02084b

Reference yield:

: 39160-70-8
3,6,9,12,15,18-hexaoxa-1-octadecyl amine

: 1264015-79-3
methyl 4-{2-[2-(2-{2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethyl}-3,5-bis[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethoxy]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 3 h / 0 °C

1.2: 20 °C

2.1: triethylamine; p-toluenesulfonyl chloride / tetrahydrofuran / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 100 °C

With potassium carbonate; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/c0cc02084b