4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

Base Information

Chemical Name:4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester
CAS No.:1316665-23-2
Molecular Formula:C₂₀H₂₂N₂O₄
Molecular Weight:354.406
Hs Code.:

Synonyms:4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

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Chemical Property of 4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

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Technology Process of 4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

There total 3 articles about 4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97-53-0
4-allylguaiacol

: 34562-97-5
N-nicotinoyl-gamma-aminobutyric acid

: 1316665-23-2
4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

Guidance literature:: With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 25 ℃; Inert atmosphere;

Reference yield:

: 59-67-6
nicotinic acid

: 1316665-23-2
4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 3 h / 25 °C / Inert atmosphere

2.1: water; lithium hydroxide / tetrahydrofuran / 25 - 45 °C

2.2: pH 2 - 3

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / N,N-dimethyl-formamide / 25 °C / Inert atmosphere

With 4-methyl-morpholine; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 4-[(pyridine-3-carbonyl)amino]butyric acid methyl ester

: 1316665-23-2
4-[(pyridine-3-carbonyl)amino]butyric acid 4-allyl-2-methoxyphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / tetrahydrofuran / 25 - 45 °C

1.2: pH 2 - 3

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / N,N-dimethyl-formamide / 25 °C / Inert atmosphere

With 4-methyl-morpholine; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;