3-fluoro-2,4-dinitrophenol

Base Information

• Chemical Name: 3-fluoro-2,4-dinitrophenol
• CAS No.: 361-47-7
• Molecular Formula: C₆H₃FN₂O₅
• Molecular Weight: 202.099
• Mol file: 361-47-7.mol

Synonyms:3-fluoro-2,4-dinitrophenol

Chemical Property of 3-fluoro-2,4-dinitrophenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-fluoro-2,4-dinitrophenol

There total 2 articles about 3-fluoro-2,4-dinitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-fluorophenol (372-20-3) + sulfuric acid (7664-93-9) → 2-nitro-3-fluorophenol (385-01-3) + 3-fluoro-2,4-dinitrophenol (361-47-7) + 3-fluoro-2,6-dinitro-phenol (361-48-8)

Guidance literature:

folgend Behandeln mit Salpeterschwefelsaeure und Destillation des Reaktionsprodukts mit Wasserdampf;

Reference yield:

3-fluorophenol (372-20-3) → 3-fluoro-2,4-dinitrophenol (361-47-7)

Guidance literature:

With sulfuric acid; at 10 - 15 ℃; nachfolgend Einw_. von Salpetersaeure und Hydrolyse des Reaktionsprodukts mit Wasserdampf;

Reference yield: 25.0%

2,2,2-trifluoroethanol (75-89-8) + 3-fluoro-2,4-dinitrophenol (361-47-7) → bis(2,2,2-trifluoroethyl) 3-fluoro-4-nitrophenyl phosphate (1361543-32-9)

Guidance literature:

3-fluoro-2,4-dinitrophenol; With triethylamine; trichlorophosphate; In chloroform; at 0 - 20 ℃; for 6h;

2,2,2-trifluoroethanol; With triethylamine; In chloroform; at 20 ℃; Cooling;

DOI:10.1002/chem.201101926

upstream raw materials:

3-fluorophenol

sulfuric acid

Downstream raw materials:

2,4-dinitroresorcinol

2,4-dinitro-1,3-phenylenediamine

bis(2,2,2-trifluoroethyl) 3-fluoro-4-nitrophenyl phosphate