[Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate)

Base Information

• Chemical Name: [Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate)
• CAS No.: 930578-76-0
• Molecular Formula: C₉H₇O₄*C₂₄H₂₆N₃NiO₆
• Molecular Weight: 690.329
• Mol file: 930578-76-0.mol

Synonyms:[Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate)

Chemical Property of [Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate)

There total 1 articles about [Ni(2-carbomethoxy benzoate)(pyridine)3(H₂O)2](2-carbomethoxy benzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

pyridine (110-86-1) + methanol (67-56-1) + phthalic anhydride (85-44-9) + nickel(II) chloride hexahydrate → [Ni(2-carbomethoxy benzoate)(pyridine)3(H2O)2](2-carbomethoxy benzoate) (930578-76-0)

Guidance literature:

With Mg; In methanol; Mg was added to soln. of anhydride in MeOH; mixt. was heated at 60°C for 3 h; cooled; soln. of Ni salt in MeOH was added; stirred at 60.ddegree.C for 2 h; filtered; filtrate evapd.; dissolved in pyridine; crystd.; elem. anal.;

DOI:10.1016/j.molstruc.2006.05.005

upstream raw materials:

pyridine

methanol

phthalic anhydride