1-(dimesitylboryl)pyrene

Base Information

Chemical Name:1-(dimesitylboryl)pyrene
CAS No.:191875-87-3
Molecular Formula:C₃₄H₃₁B
Molecular Weight:450.431
Hs Code.:

Synonyms:1-(dimesitylboryl)pyrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(dimesitylboryl)pyrene

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Technology Process of 1-(dimesitylboryl)pyrene

There total 1 articles about 1-(dimesitylboryl)pyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1714-29-0
1-bromopyrene

: 436-59-9
dimesitylfluoroborane

: 191875-87-3
1-(dimesitylboryl)pyrene

Guidance literature:: With CH₃CH₂CH₂CH₂Li; In tetrahydrofuran; diethyl ether; (N2); addn. of soln. of butyllithium to THF soln. of pyrene deriv. at -78°C for 10 min, stirring for 1 h at -78°C, addn. of ethereal soln. of boron compd., stirring at -78°C for 1 h, stirring overnight at room temp.; addn. of aq. soln. of NH4Cl, stirring for 30 min, separating organic layer, concg., chromy. (silica gel, hexanes), recrystn. (CH2Cl2/hexanes (1:1)), elem. anal.;
DOI:10.1021/om800856g