Technology Process of C26H29NO5
There total 9 articles about C26H29NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: aluminum (III) chloride / dichloromethane / 0.25 h / -5 - 0 °C
1.2: 20 h / -5 - 20 °C
2.1: potassium carbonate / acetone / 0.08 h / 20 °C
3.1: potassium carbonate / acetone / 20 - 55 °C
4.1: dichloromethane; isopropyl alcohol / 0.83 h / 0 - 5 °C
5.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C
6.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C
7.1: dimethyl sulfoxide / 2 h / 20 - 120 °C
8.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C
9.1: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C
With
aluminum (III) chloride; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol; acetone; toluene;
DOI:10.1080/00397911.2014.891745
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C
2: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C
3: dimethyl sulfoxide / 2 h / 20 - 120 °C
4: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C
5: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium hydroxide;
In
methanol; dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1080/00397911.2014.891745