[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

Base Information

Chemical Name:[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester
CAS No.:1616788-91-0
Molecular Formula:C₂₆H₂₉NO₅
Molecular Weight:435.52
Hs Code.:

Synonyms:[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

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Chemical Property of [2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

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Technology Process of [2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

There total 8 articles about [2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1616788-90-9
[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]dimethylamine

: 541-41-3
chloroformic acid ethyl ester

: 1616788-91-0
[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In toluene; at 120 ℃; for 2.5h;
DOI:10.1080/00397911.2014.891745

Reference yield:

: 90-05-1
2-methoxy-phenol

: 1616788-91-0
[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: aluminum (III) chloride / dichloromethane / 0.25 h / -5 - 0 °C

1.2: 20 h / -5 - 20 °C

2.1: potassium carbonate / acetone / 0.08 h / 20 °C

3.1: potassium carbonate / acetone / 20 - 55 °C

4.1: dichloromethane; isopropyl alcohol / 0.83 h / 0 - 5 °C

5.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C

6.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

7.1: dimethyl sulfoxide / 2 h / 20 - 120 °C

8.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

With aluminum (III) chloride; sodium tetrahydroborate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; isopropyl alcohol; acetone; toluene;
DOI:10.1080/00397911.2014.891745

Reference yield:

: 1266213-28-8
1-(4-benzyloxy-3-methoxyphenyl)-2-dimethylaminoethanone

: 1616788-91-0
[2-(4-benzyloxy-3-methoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C

2: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

3: dimethyl sulfoxide / 2 h / 20 - 120 °C

4: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; potassium hydroxide; In methanol; dimethyl sulfoxide; toluene;
DOI:10.1080/00397911.2014.891745