4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

Base Information

Chemical Name:4-[(4-methoxybenzyl)oxy]-2-methylenebutanal
CAS No.:1352739-49-1
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

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Technology Process of 4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

There total 6 articles about 4-[(4-methoxybenzyl)oxy]-2-methylenebutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.4%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 119649-27-3
4-((4-methoxybenzyl)oxy)butanal

: 1352739-49-1
4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

Guidance literature:: With N,N-dimethylammonium chloride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; at 120 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2018.12.010

Reference yield: 45.0%

: 250209-01-9
4-hydroxy-2-methylenebutanal

: 4-methoxyphenyl 2,2,2-trichloroacetimidate

: 1352739-49-1
4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; cyclohexane; for 10h; Inert atmosphere;
DOI:10.1002/ejoc.201100669

Reference yield:

: 55881-94-2
3-methylene-1,4-dihydroxybutane

: 1352739-49-1
4-[(4-methoxybenzyl)oxy]-2-methylenebutanal

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen; palladium diacetate; triethylamine / tetrahydrofuran; toluene

2: camphor-10-sulfonic acid / dichloromethane; cyclohexane / 10 h / Inert atmosphere

With camphor-10-sulfonic acid; oxygen; palladium diacetate; triethylamine; In tetrahydrofuran; dichloromethane; cyclohexane; toluene;
DOI:10.1002/ejoc.201100669