bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

Base Information

Chemical Name:bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether
CAS No.:181725-55-3
Molecular Formula:C₆₂H₇₆N₂O₁₃
Molecular Weight:1057.29
Hs Code.:

Synonyms:bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

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Chemical Property of bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

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Technology Process of bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

There total 11 articles about bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 181725-53-1
2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

: 181725-55-3
bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

Guidance literature:: With sodium hydroxide; tetraethylammonium bromide; In dichloromethane; for 72h;
DOI:10.1055/s-1996-4319

Reference yield:

: 24878-25-9
bis(2-aminophenyl)ether

: 181725-55-3
bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

2: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

3: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

4: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

5: 81 percent / Et₄NBr, aq. NaOH / CH₂Cl₂ / 72 h

With sodium hydroxide; lithium aluminium tetrahydride; tetraethylammonium bromide; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319

Reference yield:

: 2217-65-4
bis(2-nitrophenyl)ether

: 181725-55-3
bis[2-{2-[N-benzyl-2-(tert-butoxycarbonyl)ethoxy]phenoxy}ethoxyethylaminophenyl] ether

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / NH₂NH₂*H₂O / 10percent Pd/C / ethanol / 1 h / Heating

2: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

3: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

4: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

5: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

6: 81 percent / Et₄NBr, aq. NaOH / CH₂Cl₂ / 72 h

With sodium hydroxide; lithium aluminium tetrahydride; tetraethylammonium bromide; hydrogen; sodium hydride; hydrazine hydrate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319