2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

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Chemical Name:2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol
CAS No.:181725-53-1
Molecular Formula:C₅₀H₅₆N₂O₉
Molecular Weight:829.003
Hs Code.:

Synonyms:2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

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Chemical Property of 2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

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Technology Process of 2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

There total 10 articles about 2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 181725-51-9
N-Benzyl-N-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-acetyl)-amino]-phenoxy}-phenyl)-2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-acetamide

: 181725-53-1
2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 16h; Heating;
DOI:10.1055/s-1996-4319

Reference yield:

: 24878-25-9
bis(2-aminophenyl)ether

: 181725-53-1
2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

2: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

3: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

4: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

With lithium aluminium tetrahydride; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319

Reference yield:

: 2217-65-4
bis(2-nitrophenyl)ether

: 181725-53-1
2-[4-(2-{2-[Benzyl-(2-{2-[benzyl-(2-{2-[4-(2-hydroxy-ethoxy)-phenoxy]-ethoxy}-ethyl)-amino]-phenoxy}-phenyl)-amino]-ethoxy}-ethoxy)-phenoxy]-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / NH₂NH₂*H₂O / 10percent Pd/C / ethanol / 1 h / Heating

2: 65 percent / Et₃N / CH₂Cl₂ / 2 h / Heating

3: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, 16 h

4: 92 percent / H₂ / 10percent Pd/C / ethanol / 16 h / Ambient temperature

5: 44 percent / LiAlH₄ / tetrahydrofuran / 16 h / Heating

With lithium aluminium tetrahydride; hydrogen; sodium hydride; hydrazine hydrate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1055/s-1996-4319