2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

Base Information

Chemical Name:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt
CAS No.:1278584-02-3
Molecular Formula:C₄H₁₁NO₃*C₂₅H₃₁ClN₂O₇S
Molecular Weight:660.186
Hs Code.:

2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

Synonyms:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

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Chemical Property of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

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Technology Process of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

There total 6 articles about 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

: 77-86-1
2-amino-2-hydroxymethyl-1,3-propanediol

: 1278584-02-3
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

Guidance literature:: In water; acetone; at 60 ℃;

Reference yield:

: 1187857-74-4
N-(4-chlorophenyl)-N-phenyl-1H-imidazole-1-carboxamide

: 1278584-02-3
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

2.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

2.3: pH 7 - 8

3.1: thionyl chloride / 20 °C

4.1: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

5.1: water; acetone / 60 °C

With thionyl chloride; tetrabutylammomium bromide; water; sodium hydroxide; In tetrahydrofuran; water; acetone; toluene; acetonitrile;

Reference yield:

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

: 1278584-02-3
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid tris(hydroxymethyl)aminomethane salt

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 20 °C

2: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

3: water; acetone / 60 °C

With thionyl chloride; sodium hydroxide; In tetrahydrofuran; water; acetone;