sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Base Information

Chemical Name:sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate
CAS No.:1187856-43-4
Molecular Formula:C₂₃H₂₅ClNO₅*Na
Molecular Weight:453.898
Hs Code.:

Synonyms:sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Chemical Property:

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Technology Process of sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

There total 12 articles about sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187856-46-7
tert-butyl 2-(((1r,4r)-4-(((4-chlorophenyl)-(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

: 1310-73-2
sodium hydroxide

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: tert-butyl 2-(((1r,4r)-4-(((4-chlorophenyl)-(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃;

sodium hydroxide; In methanol; Cooling with ice bath;

Reference yield:

: 1205-71-6
N-(4-chlorophenyl)aniline

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate / acetonitrile / 5.5 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

3.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

3.3: pH 7 - 8

With potassium phosphate; tetrabutylammomium bromide; water; sodium hydroxide; In toluene; acetonitrile;

Reference yield:

: 1187857-74-4
N-(4-chlorophenyl)-N-phenyl-1H-imidazole-1-carboxamide

: 1187856-43-4
sodium 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

2.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

2.3: pH 7 - 8

With tetrabutylammomium bromide; water; sodium hydroxide; In toluene; acetonitrile;