Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Base Information

Chemical Name:Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid
CAS No.:86443-85-8
Molecular Formula:C₃₄H₃₉N₉O₈
Molecular Weight:701.739
Hs Code.:

Synonyms:Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

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Chemical Property of Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

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Technology Process of Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

There total 4 articles about Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 86319-53-1
Methyl-6-O-(6-O-Acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

: 86443-85-8
Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: With sodium methylate; In methanol; for 0.5h; Heating;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 61135-12-4
6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-α-D-glucopyranosylbromid

: 86443-85-8
Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / molecular sieve, silver carbonate / CH₂Cl₂ / 0.08 h

2: 97 percent / sodium methoxide / methanol / 0.5 h / Heating

3: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

4: 99 percent / sodium methanolate / methanol / 0.5 h / Heating

With molecular sieve; sodium methylate; silver carbonate; mercury dibromide; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90950-9

Reference yield:

: 86319-52-0
Methyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

: 86443-85-8
Methyl-2,4-diazido-6-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) mercury (II) bromide, molecular sieve / 1.) CH₂Cl₂, 1 h, r.t.; 2.) CH₂Cl₂, -40 deg C, 6.5 h

2: 99 percent / sodium methanolate / methanol / 0.5 h / Heating

With molecular sieve; sodium methylate; mercury dibromide; In methanol;
DOI:10.1016/S0008-6215(00)90950-9