5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

Base Information

Chemical Name:5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one
CAS No.:1372192-32-9
Molecular Formula:C₂₉H₃₃NO₇S₂
Molecular Weight:571.716
Hs Code.:

Synonyms:5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

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Chemical Property of 5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

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Technology Process of 5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

There total 7 articles about 5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372195-75-9
methyl 3-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

: 1372192-32-9
5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 1h;

Reference yield:

: 1000413-85-3
(2’,6’-dimethyl-4’-(3-(methylsulfonyl)propoxy)-[1,1‘-biphenyl]-3-yl)methanol

: 1372192-32-9
5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid; hydrogen bromide / 3.5 h / 60 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / Cooling

3.2: Cooling

3.3: 20 °C / Cooling

4.1: sodium methylate / tetrahydrofuran; methanol / 0.17 h / 20 °C

4.2: 65 h / Reflux

5.1: sodium chloride / N,N-dimethyl-formamide / 17 h / Reflux

6.1: acetic acid / water / 3 h / 80 °C

7.1: sodium methylate / methanol / 1 h / 20 °C

With sulfuric acid; hydrogen bromide; sodium methylate; potassium carbonate; acetic acid; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1372195-73-7
dimethyl 2-(2-(N,N-bis(2-(trimethylsilyl)ethoxymethyl)sulfamoyl)-1-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)ethyl)malonate

: 1372192-32-9
5-[4-[[3-[2,6-dimethyl-4-(3-methylsulfonylpropoxy)phenyl]phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium chloride / N,N-dimethyl-formamide / 17 h / Reflux

2: acetic acid / water / 3 h / 80 °C

3: sodium methylate / methanol / 1 h / 20 °C

With sodium methylate; acetic acid; sodium chloride; In methanol; water; N,N-dimethyl-formamide;