(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

Base Information

Chemical Name:(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide
CAS No.:1372195-72-6
Molecular Formula:C₃₉H₅₉NO₈S₂Si₂
Molecular Weight:790.202
Hs Code.:

Synonyms:(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

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Chemical Property of (E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

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Technology Process of (E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

There total 4 articles about (E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372195-70-4
N,N-bis((2-(trimethylsilyl)ethoxy)methyl)methanesulfonamide

: 1372195-71-5
4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)benzaldehyde

: 1372195-72-6
(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

Guidance literature:: N,N-bis((2-(trimethylsilyl)ethoxy)methyl)methanesulfonamide; With lithium hexamethyldisilazane; In tetrahydrofuran; Cooling;

With diethyl chlorophosphate; In tetrahydrofuran; Cooling;

4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)benzaldehyde; In tetrahydrofuran; at 20 ℃; Cooling;

Reference yield:

: 1000413-85-3
(2’,6’-dimethyl-4’-(3-(methylsulfonyl)propoxy)-[1,1‘-biphenyl]-3-yl)methanol

: 1372195-72-6
(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; hydrogen bromide / 3.5 h / 60 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / Cooling

3.2: Cooling

3.3: 20 °C / Cooling

With sulfuric acid; hydrogen bromide; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1372194-98-3
3‘-(bromomethyl)-2,6-dimethyl-4-(3-(methylsulfonyl)propoxy)-1,1‘-biphenyl

: 1372195-72-6
(E)-2-(4-((2',6'-dimethyl-4'-(3-(methylsulfonyl)propoxy)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis((2-(trimethylsilyl)ethoxy)methyl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / Cooling

2.2: Cooling

2.3: 20 °C / Cooling

With potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide;