N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Base Information

Chemical Name:N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin
CAS No.:15778-68-4
Molecular Formula:C₃₁H₃₁NO₄
Molecular Weight:481.591
Hs Code.:

Synonyms:N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Suppliers and Price of N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Chemical Property:

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Technology Process of N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

There total 6 articles about N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 22231-61-4
2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine

: 15778-68-4
N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Guidance literature:: With 4 A molecular sieve; In methanol; for 3h; Heating;
DOI:10.1021/jo020010d

Reference yield:

: 100-39-0
benzyl bromide

: 15778-68-4
N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / K₂CO₃ / ethanol

2: 68 percent / NH₄OAc / acetic acid / 4 h / Heating

3: 71 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

4: 97 percent / 4 Angstroem molecular sieves / methanol / 3 h / Heating

With lithium aluminium tetrahydride; 4 A molecular sieve; ammonium acetate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; ethanol; acetic acid;
DOI:10.1021/jo020010d

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 15778-68-4
N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / K₂CO₃ / ethanol

2: 68 percent / NH₄OAc / acetic acid / 4 h / Heating

3: 71 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

4: 97 percent / 4 Angstroem molecular sieves / methanol / 3 h / Heating

With lithium aluminium tetrahydride; 4 A molecular sieve; ammonium acetate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; ethanol; acetic acid;
DOI:10.1021/jo020010d