N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Base Information

Chemical Name:N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine
CAS No.:15778-71-9
Molecular Formula:C₃₁H₃₃NO₄
Molecular Weight:483.607
Hs Code.:

Synonyms:N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

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Chemical Property of N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Chemical Property:

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Technology Process of N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

There total 7 articles about N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 15778-68-4
N-<4-Benzyloxy-3-methoxy-benzyliden>-4-benzyloxy-3-methoxy-phenaethylamin

: 15778-71-9
N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃;
DOI:10.1021/jo020010d

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 15778-71-9
N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / NH₄OAc / acetic acid / 4 h / Heating

2: 71 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

3: 97 percent / 4 Angstroem molecular sieves / methanol / 3 h / Heating

4: 65 percent / NaBH₄ / methanol / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; 4 A molecular sieve; ammonium acetate; In tetrahydrofuran; methanol; diethyl ether; acetic acid;
DOI:10.1021/jo020010d

Reference yield:

: 100-39-0
benzyl bromide

: 15778-71-9
N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / K₂CO₃ / ethanol

2: 68 percent / NH₄OAc / acetic acid / 4 h / Heating

3: 71 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 2 h / Heating

4: 97 percent / 4 Angstroem molecular sieves / methanol / 3 h / Heating

5: 65 percent / NaBH₄ / methanol / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; 4 A molecular sieve; ammonium acetate; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; ethanol; acetic acid;
DOI:10.1021/jo020010d