(1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide

Base Information

• Chemical Name: (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide
• CAS No.: 118599-39-6
• Molecular Formula: C₂₃H₂₂O₄
• Molecular Weight: 362.425

Synonyms:(1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide

Chemical Property of (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide

Chemical Property:

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Technology Process of (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide

There total 2 articles about (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

1,3-diphenyl-2-methyl-1-H-indene (51310-26-0) → 1-(2-Benzoyl-phenyl)-1-phenyl-propan-2-one (118599-35-2) + (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide (118599-39-6) + (1S,8S,9R)-9-Methyl-1,8-diphenyl-10,11,12-trioxa-tricyclo[7.2.1.02,7]dodeca-2,4,6-triene (89619-60-3,89675-15-0,118710-99-9,118711-02-7)

Guidance literature:

With ozone; In methanol; dichloromethane; at -70 ℃;

DOI:10.1021/ja00187a038

Reference yield: 21.0%

methanol (67-56-1) + 1,3-diphenyl-2-methyl-1-H-indene (51310-26-0) → 1-(2-Benzoyl-phenyl)-1-phenyl-propan-2-one (118599-35-2) + (1R,3R,4S)-1-Methoxy-3-methyl-1,4-diphenyl-isochroman-3-yl-hydroperoxide (118599-39-6) + (1S,8S,9R)-9-Methyl-1,8-diphenyl-10,11,12-trioxa-tricyclo[7.2.1.02,7]dodeca-2,4,6-triene (89619-60-3,89675-15-0,118710-99-9,118711-02-7)

Guidance literature:

With ozone; In dichloromethane; at -70 ℃;

DOI:10.1021/ja00187a038

upstream raw materials:

methanol

1,3-diphenyl-2-methyl-1-H-indene

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