Gly-Ni-PABP

Base Information

Chemical Name:Gly-Ni-PABP
CAS No.:124302-98-3
Molecular Formula:C₂₁H₁₅N₃O₃*Ni
Molecular Weight:416.058
Hs Code.:

Synonyms:Gly-Ni-PABP

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Gly-Ni-PABP

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Technology Process of Gly-Ni-PABP

There total 5 articles about Gly-Ni-PABP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124522-52-7
pyridine-2-carboxylic acid(2-benzoyl-phenyl)-amide

: 56-40-6,18875-39-3,25718-94-9
glycine

: nickel(II) nitrate

: 124302-98-3
(N-{phenyl[2-(pyridine-2-carboxamido)phenyl]methylidene}glycinato-N,N',N'',O)nickel(II)

Guidance literature:: With potassium hydroxide; sodium methylate; In methanol; glycine, Ni(NO3)2 and amide were reacted in presence of KOH or MeONa in methanol; chromd. or crystd. from CHCl3;
DOI:10.1021/ja035465e

Reference yield: 91.0%

: nickel(II) nitrate hexahydrate

: 124522-52-7
pyridine-2-carboxylic acid(2-benzoyl-phenyl)-amide

: 56-40-6,18875-39-3,25718-94-9
glycine

: 124302-98-3
(N-{phenyl[2-(pyridine-2-carboxamido)phenyl]methylidene}glycinato-N,N',N'',O)nickel(II)

Guidance literature:: With sodium methylate; In methanol; condensation of C19H14N2O2, Ni(NO3)2*6H2O, and glycine under reflux for 20 min; crystd. from CHCl3; detd. by elem. anal., NMR, UV, IR;
DOI:10.1002/1521-3773(20010518)40:10<1948::AID-ANIE1948>3.0.CO;2-O