7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

Base Information

Chemical Name:7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one
CAS No.:1352798-45-8
Molecular Formula:C₁₃H₁₀Cl₂N₄O₂
Molecular Weight:325.154
Hs Code.:

Synonyms:7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

Chemical Property:

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Technology Process of 7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

There total 7 articles about 7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39183-17-0
4-hydroxy-2,3-dichloroaniline

: 1352798-45-8
7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

1.2: 19 h / 20 °C

2.1: iron; acetic acid / 1.5 h / 55 °C

3.1: pyridine / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C

With pyridine; iron; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1352798-46-9
C₁₅H₁₆Cl₂N₄O₃

: 1352798-45-8
7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 22h; Inert atmosphere;

Reference yield:

: 1352798-56-1
ethyl (2-amino-4-(4-amino-2,3-dichlorophenoxy)pyridin-3-yl)carbamate

: 74-88-4
methyl iodide

: 1352798-45-8
7-(4-amino-2,3-dichlorophenoxy)-1-methyl-1H-imidazo[4,5-b]pyridin-2(3H)-one

Guidance literature:: ethyl (2-amino-4-(4-amino-2,3-dichlorophenoxy)pyridin-3-yl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.75h; Inert atmosphere;

methyl iodide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;