4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

Base Information

• Chemical Name: 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene
• CAS No.: 1313583-15-1
• Molecular Formula: C₂₆H₃₉NO₉
• Molecular Weight: 509.597

Synonyms:4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

Chemical Property of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

Chemical Property:

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Technology Process of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

There total 3 articles about 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene (1313583-14-0) → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene (1313583-15-1)

Guidance literature:

With nitric acid; silica gel; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/ja2016125

Reference yield:

2-bromoethyl triethylene glycol adamantyl ether → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene (1313583-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / acetone / 48 h / Reflux

2: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

With nitric acid; silica gel; caesium carbonate; In dichloromethane; acetone;

DOI:10.1021/ja2016125

Reference yield:

1,3-dimethoxy-2-hydroxy-benzene (91-10-1) → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene (1313583-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / acetone / 48 h / Reflux

2: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

With nitric acid; silica gel; caesium carbonate; In dichloromethane; acetone;

DOI:10.1021/ja2016125

upstream raw materials:

1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

1,3-dimethoxy-2-hydroxy-benzene

Downstream raw materials:

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

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