4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

Base Information

• Chemical Name: 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline
• CAS No.: 1313583-16-2
• Molecular Formula: C₂₆H₄₁NO₇
• Molecular Weight: 479.614

Synonyms:4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

Chemical Property of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

Chemical Property:

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Technology Process of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

There total 4 articles about 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene (1313583-15-1) → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline (1313583-16-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 4h; under 750.075 Torr;

DOI:10.1021/ja2016125

Reference yield:

2-bromoethyl triethylene glycol adamantyl ether → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline (1313583-16-2)

Guidance literature:

Multi-step reaction with 3 steps

1: caesium carbonate / acetone / 48 h / Reflux

2: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 750.08 Torr

With palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; caesium carbonate; In methanol; dichloromethane; acetone;

DOI:10.1021/ja2016125

Reference yield:

1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene (1313583-14-0) → 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline (1313583-16-2)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 750.08 Torr

With palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; In methanol; dichloromethane;

DOI:10.1021/ja2016125

upstream raw materials:

1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

1,3-dimethoxy-2-hydroxy-benzene

Downstream raw materials:

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

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