1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

Base Information

Chemical Name:1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene
CAS No.:1313583-14-0
Molecular Formula:C₂₆H₄₀O₇
Molecular Weight:464.599
Hs Code.:

Synonyms:1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

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Chemical Property of 1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

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Technology Process of 1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

There total 1 articles about 1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2-bromoethyl triethylene glycol adamantyl ether

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 1313583-14-0
1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

Guidance literature:: With caesium carbonate; In acetone; for 48h; Reflux;
DOI:10.1021/ja2016125

Reference yield: 97.0%

: 1313583-14-0
1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

: 1313583-15-1
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxy-1-nitrobenzene

Guidance literature:: With nitric acid; silica gel; In dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1021/ja2016125

Reference yield:

: 1313583-14-0
1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

: 1313583-16-2
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 750.08 Torr

With palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; In methanol; dichloromethane;
DOI:10.1021/ja2016125