4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

Base Information

Chemical Name:4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide
CAS No.:1313583-21-9
Molecular Formula:C₄₅H₇₇NO₁₆S
Molecular Weight:920.169
Hs Code.:

4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

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Chemical Property of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

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Technology Process of 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

There total 5 articles about 4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 866889-02-3
1-mercapto-3,6,9,12,15,18,21,24-octaoxaheptacosan-27-oic acid

: 1313583-16-2
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyaniline

: 1313583-21-9
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ja2016125

Reference yield:

: 2-bromoethyl triethylene glycol adamantyl ether

: 1313583-21-9
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / acetone / 48 h / Reflux

2: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 750.08 Torr

4: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

With palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; caesium carbonate; dicyclohexyl-carbodiimide; In methanol; dichloromethane; acetone;
DOI:10.1021/ja2016125

Reference yield:

: 1313583-14-0
1-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-2,6-dimethoxybenzene

: 1313583-21-9
4-[2-(2-{2-[2-(adamantan-1-yloxy)ethoxy]ethoxy}ethoxy)ethoxy]-3,5-dimethoxyphenyl O-(carboxyethyl)-O'-(2-mercaptoethyl)-heptaethylene glycol amide

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; silica gel / dichloromethane / 0.08 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 750.08 Torr

3: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

With palladium 10% on activated carbon; hydrogen; nitric acid; silica gel; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja2016125