furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

Base Information

Chemical Name:furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide
CAS No.:1443221-54-2
Molecular Formula:C₂₀H₁₃N₃O₃S
Molecular Weight:375.408
Hs Code.:

Synonyms:furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

Suppliers and Price of furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

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Technology Process of furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

There total 5 articles about furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 6221-12-1
3-Bromoacetylpyridine

: 952612-06-5
1-[1-diethylamino-1-phenylmeth-(Z)-ylidene]-3-(furan-2-carbonyl)thiourea

: 1443221-54-2
furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2013.03.020

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 1443221-54-2
furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide / benzene / 20 °C

2: ethyl acetate; Petroleum ether / 3 h / -5 - 5 °C

3: N,N-dimethyl-formamide / 24 h / 20 °C

With tetrabutylammomium bromide; In ethyl acetate; N,N-dimethyl-formamide; Petroleum ether; benzene;
DOI:10.1016/j.ejmech.2013.03.020

Reference yield:

: 100-47-0
benzonitrile

: 1443221-54-2
furan-2-carboxylic-acid [4-phenyl-5-(pyridine-3-carbonyl)thiazol-2-yl]amide

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 0 - 30 °C

2: ethyl acetate; Petroleum ether / 3 h / -5 - 5 °C

3: N,N-dimethyl-formamide / 24 h / 20 °C

With aluminum (III) chloride; In ethyl acetate; N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1016/j.ejmech.2013.03.020