(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

Base Information

Chemical Name:(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate
CAS No.:1380572-83-7
Molecular Formula:C₁₆H₈Cl₅F₃O₃
Molecular Weight:482.498
Hs Code.:

Synonyms:(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

Suppliers and Price of (2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of (2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

There total 3 articles about (2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380572-68-8
3-[(2,6-dichloro-4-methoxy-phenyl)-(2,4,6-trichloro-phenyl)-methoxymethyl]-1-(3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione

: 76-05-1
trifluoroacetic acid

: 1380572-83-7
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

: 58-96-8
uridine

Guidance literature:: In dichloromethane; for 2h;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-66-6
(((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl) methyl sulfide

: 1380572-83-7
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

3: dichloromethane / 2 h

With sulfuryl dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-67-7
((2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methoxy)methyl chloride

: 1380572-83-7
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methyl 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

2: dichloromethane / 2 h

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.03.121