Technology Process of C30H44N8O4
There total 15 articles about C30H44N8O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-(3-((((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl)amino)propyl)-3-(4-(tert-butyl)phenyl)urea; acetone;
With
acetic acid;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 6h;
4 A Molecular sieve;
With
sodium cyanoborohydride;
In
tetrahydrofuran; methanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
2.1: acetic acid / tetrahydrofuran; methanol / 6 h / 20 °C / 4 A Molecular sieve
2.2: 20 °C
With
sodium tris(acetoxy)borohydride; acetic acid;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / water
1.2: 1 h
1.3: pH 8
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
3.1: hydrazine hydrate / ethanol / 3 h / 20 °C / Reflux
4.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
5.1: acetic acid / tetrahydrofuran; methanol / 6 h / 20 °C / 4 A Molecular sieve
5.2: 20 °C
With
sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; water; 1,2-dichloro-ethane;