C₁₈H₂₂O₆

Base Information

Chemical Name:C₁₈H₂₂O₆
CAS No.:1415636-81-5
Molecular Formula:C₁₈H₂₂O₆
Molecular Weight:334.369
Hs Code.:

C<sub>18</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:C₁₈H₂₂O₆

Suppliers and Price of C₁₈H₂₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₁₈H₂₂O₆

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of C₁₈H₂₂O₆

There total 13 articles about C₁₈H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₄O₇

: 1415636-81-5
C₁₈H₂₂O₆

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; In chloroform; at -15 ℃; for 0.5h;
DOI:10.1021/ol302842h

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1415636-81-5
C₁₈H₂₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere

1.2: 24 h / 25 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 0 °C

2.2: 20 °C

3.1: lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane / 2 h / 80 °C

4.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / 0 °C

5.1: tetrahydrofuran / 1 h / 0 °C

6.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₄₂N₂; potassium tert-butylate; hydrogen / propan-1-ol / 0.25 h / 25 °C / 4560.31 Torr / Inert atmosphere; Autoclave

7.1: trimethylpyruvic acid / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C

8.1: ozone / methanol / 3 h / -78 °C

9.1: sodium tetrahydroborate / methanol; water / 1 h / 25 °C / Inert atmosphere

10.1: sodium hydroxide; water / methanol / 1 h / 25 °C

11.1: triethylamine; chloroformic acid ethyl ester / chloroform / 0.5 h / -15 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₄₂N₂; potassium tert-butylate; water; hydrogen; isopropylmagnesium chloride; chloroformic acid ethyl ester; sodium hydride; sodium carbonate; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; trimethylpyruvic acid; lithium chloride; sodium hydroxide; In tetrahydrofuran; methanol; propan-1-ol; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; chloroform; water; 7.1: |Johnson-Claisen Rearrangement;
DOI:10.1021/ol302842h

Reference yield:

: 52506-21-5
8-oxo-1,4-dioxa-spiro[4.5]decane-7-carboxylic acid methyl ester

: 1415636-81-5
C₁₈H₂₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 0 °C

1.2: 20 °C

2.1: lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane / 2 h / 80 °C

3.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / 0 °C

4.1: tetrahydrofuran / 1 h / 0 °C

5.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₄₂N₂; potassium tert-butylate; hydrogen / propan-1-ol / 0.25 h / 25 °C / 4560.31 Torr / Inert atmosphere; Autoclave

6.1: trimethylpyruvic acid / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C

7.1: ozone / methanol / 3 h / -78 °C

8.1: sodium tetrahydroborate / methanol; water / 1 h / 25 °C / Inert atmosphere

9.1: sodium hydroxide; water / methanol / 1 h / 25 °C

10.1: triethylamine; chloroformic acid ethyl ester / chloroform / 0.5 h / -15 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₄₂N₂; potassium tert-butylate; water; hydrogen; isopropylmagnesium chloride; chloroformic acid ethyl ester; sodium carbonate; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; trimethylpyruvic acid; lithium chloride; sodium hydroxide; In tetrahydrofuran; methanol; propan-1-ol; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; chloroform; water; 6.1: |Johnson-Claisen Rearrangement;
DOI:10.1021/ol302842h