2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester

Base Information

• Chemical Name: 2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester
• CAS No.: 1584706-01-3
• Molecular Formula: C₉₄H₁₄₃N₃O₉
• Molecular Weight: 1459.18

Synonyms:2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester

Chemical Property of 2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester

Chemical Property:

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Technology Process of 2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester

There total 1 articles about 2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-amino-5-(dodecyloxy)phenol (863432-10-4) + 2,3-bis-(3,4-didodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-formyl-3-hydroxy phenyl ester → 2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester (1584706-01-3)

Guidance literature:

In ethanol; for 3h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2014.02.030

Reference yield: 90.0%

2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester (1584706-01-3) + zinc diacetate (557-34-6) → bis{2,3-bis(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]-3-hydroxyphenyl ester}zinc(II) (1584706-09-1)

Guidance literature:

In tetrahydrofuran; ethanol; for 2h; Reflux;

DOI:10.1016/j.tet.2014.02.030

Reference yield: 89.0%

2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)-methyl]-3-hydroxyphenyl ester (1584706-01-3) + copper(II) acetate monohydrate (6046-93-1) → bis{2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]-3-hydroxyphenyl ester}copper(II) (1584706-08-0)

Guidance literature:

In tetrahydrofuran; ethanol; for 2h; Reflux;

DOI:10.1016/j.tet.2014.02.030

upstream raw materials:

2-amino-5-(dodecyloxy)phenol

Downstream raw materials:

bis{2,3-bis-(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]-3-hydroxyphenyl ester}copper(II)

{2,3-bis(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]-3-hydroxyphenyl ester} palladium(II)

bis{2,3-bis(3,4-bis-dodecyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]-3-hydroxyphenyl ester}zinc(II)

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