(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

Base Information

Chemical Name:(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea
CAS No.:1413176-40-5
Molecular Formula:C₂₁H₃₆N₂O₃Si
Molecular Weight:392.614
Hs Code.:

Synonyms:(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

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Chemical Property of (S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

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Technology Process of (S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

There total 3 articles about (S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.1%

: 1413176-34-7
(S)-1-(tert-butyldimethylsilyloxy)-N-(4-methoxybenzyl)propan-2-amine

: 1476-23-9
allylisocyanate

: 1413176-40-5
(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

Guidance literature:: In tetrahydrofuran; Cooling with ice;
DOI:10.1039/c2cc35484e

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1413176-40-5
(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 3 h / 20 °C / Molecular sieve

1.2: 2 h / 20 °C

2.1: triethylamine / dichloromethane / 12 h / 20 °C

3.1: tetrahydrofuran / Cooling with ice

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc35484e

Reference yield:

: 570398-18-4
(2S)-2-[[(4-methoxyphenyl)methyl]amino]propan-1-ol

: 1413176-40-5
(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: tetrahydrofuran / Cooling with ice

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc35484e