(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

Base Information

Chemical Name:(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate
CAS No.:1413176-48-3
Molecular Formula:C₂₆H₄₄N₂O₅Si
Molecular Weight:492.731
Hs Code.:

Synonyms:(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

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Chemical Property of (S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

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Technology Process of (S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

There total 4 articles about (S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: 1413176-40-5
(S)-3-allyl-1-(1-(tert-butyldimethylsilyloxy)propan-2-yl)-1-(4-methoxybenzyl)urea

: 1538-75-6
2,2-dimethylpropanoic anhydride

: 1413176-48-3
(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 0 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1039/c2cc35484e

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1413176-48-3
(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 3 h / 20 °C / Molecular sieve

1.2: 2 h / 20 °C

2.1: triethylamine / dichloromethane / 12 h / 20 °C

3.1: tetrahydrofuran / Cooling with ice

4.1: dmap; triethylamine / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux

With dmap; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc35484e

Reference yield:

: 570398-18-4
(2S)-2-[[(4-methoxyphenyl)methyl]amino]propan-1-ol

: 1413176-48-3
(S)-tert-butyl allyl((1-(tert-butyldimethylsilyloxy)propan-2-yl)(4-methoxybenzyl)carbamoyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: tetrahydrofuran / Cooling with ice

3: dmap; triethylamine / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere; Reflux

With dmap; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc35484e