C₃₀H₂₉Cl₅N₂O₈

Base Information

Chemical Name:C₃₀H₂₉Cl₅N₂O₈
CAS No.:1380572-74-6
Molecular Formula:C₃₀H₂₉Cl₅N₂O₈
Molecular Weight:722.834
Hs Code.:

C<sub>30</sub>H<sub>29</sub>Cl<sub>5</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₀H₂₉Cl₅N₂O₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₂₉Cl₅N₂O₈

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Technology Process of C₃₀H₂₉Cl₅N₂O₈

There total 10 articles about C₃₀H₂₉Cl₅N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1380572-73-5
C₄₉H₄₃Cl₅N₂O₈

: 1380572-74-6
C₃₀H₂₉Cl₅N₂O₈

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; chemoselective reaction;
DOI:10.1016/j.tet.2012.03.121

Reference yield: 80.0%

: 1380572-72-4
C₃₆H₄₃Cl₅N₂O₈Si

: 1380572-74-6
C₃₀H₂₉Cl₅N₂O₈

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 20 ℃; for 5h; chemoselective reaction;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-64-4
(2,6-dichloro-4-methoxyphenyl)(2,4,6-trichlorophenyl)methanone

: 1380572-74-6
C₃₀H₂₉Cl₅N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 3 h / 0 °C

3.1: sulfuryl dichloride / dichloromethane / 1 h / 20 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0 °C

5.1: 1H-imidazole / dichloromethane / 4 h

6.1: N-Bromosuccinimide; boron trifluoride diethyl etherate / acetonitrile / 0.25 h / 20 °C / Darkness

7.1: hydrogen fluoride / acetonitrile / 5 h / 20 °C

With 1H-imidazole; N-Bromosuccinimide; lithium borohydride; sulfuryl dichloride; boron trifluoride diethyl etherate; hydrogen fluoride; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.tet.2012.03.121