pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Base Information

• Chemical Name: pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside
• CAS No.: 960205-52-1
• Molecular Formula: C₆₀H₇₈O₁₄
• Molecular Weight: 1023.27

Synonyms:pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Chemical Property of pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

There total 3 articles about pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

pent-4-enyl 3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-58-7) + pivaloyl chloride (3282-30-2) → pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-52-1)

Guidance literature:

In pyridine; at 20 ℃; for 1.5h;

DOI:10.1021/jo701349c

Reference yield: 49.0%

dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate (943439-96-1) + 8-(4,4'-dimethoxytrityloxy)oct-4(Z)-en-1-ol (253683-39-5) + dibutyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranoside phosphate (943837-19-2) + diisopropyl-(1H,1H,2H,2H-perfluorodecyl)silyl triflate (404942-40-1) → pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranoside (960205-54-3) + pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-52-1) + pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-50-9) + pent-4-enyl 3,4-di-O-benzyl-6-O-{(1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluorodecyl)diisopropylsilyl}-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Guidance literature:

Multistep reaction.;

DOI:10.1021/jo701349c

Reference yield:

dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate (943439-96-1) + 8-(4,4'-dimethoxytrityloxy)oct-4(Z)-en-1-ol (253683-39-5) + dibutyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranoside phosphate (943837-19-2) → pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranoside (960205-54-3) + pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-52-1) + pent-4-en-1-yl 3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-56-5) + pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside (960205-50-9)

Guidance literature:

Multistep reaction.;

DOI:10.1021/jo701349c

upstream raw materials:

dibutyl 3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-2-O-pivaloyl-β-D-glucopyranoside phosphate

8-(4,4'-dimethoxytrityloxy)oct-4(Z)-en-1-ol

dibutyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranoside phosphate

diisopropyl-(1H,1H,2H,2H-perfluorodecyl)silyl triflate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 960205-52-1 pent-4-enyl 3,4-di-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-(1->6)-3,4-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send