N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide
• CAS No.: 1094359-05-3
• Molecular Formula: C₁₇H₂₅NO₄S
• Molecular Weight: 339.456

Synonyms:N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide

Chemical Property of N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide

There total 2 articles about N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-Methoxypropene (116-11-0) + N-(2,2-bis(hydroxymethyl)pent-4-en-1-yl)-4-methylbenzenesulfonamide (1094359-57-5) → N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide (1094359-05-3)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja806585m

Reference yield:

C10H19NO2 (1094359-55-3) + p-toluenesulfonyl chloride (98-59-9) → N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide (1094359-05-3)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/ja806585m

Reference yield: 72.0%

[bis(acetoxy)iodo]benzene (3240-34-4) + N-(5-allyl-2,2-dimethyl-[1,3]dioxan-5-ylmethyl)-4-methyl-benzenesulfonamide (1094359-05-3) → C19H27NO6S + C19H27NO6S

Guidance literature:

With C₂₇H₂₂N₂O; palladium diacetate; at 0 ℃; for 18h; enantioselective reaction;

DOI:10.1021/jacs.8b03767

upstream raw materials:

C₁₀H₁₉NO₂

p-toluenesulfonyl chloride

2-Methoxypropene

N-(2,2-bis(hydroxymethyl)pent-4-en-1-yl)-4-methylbenzenesulfonamide

Downstream raw materials:

8,8-dimethyl-3-(2,2,6,6-tetramethyl-piperidin-1-yloxymethyl)-2-(toluene-4-sulfonyl)-7,9-dioxa-2-aza-spiro[4.5]decane

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