6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine

Base Information

• Chemical Name: 6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine
• CAS No.: 886224-36-8
• Molecular Formula: C₁₂H₈F₃N₅O₂
• Molecular Weight: 311.223

Synonyms:6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine

Chemical Property of 6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine

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Technology Process of 6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine

There total 1 articles about 6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

1-Phenyl-4,4,4-trifluorobutane-1,3-dione (326-06-7) + 3-amino-1,2,4-triazole (61-82-5) → 6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine (886224-36-8)

Guidance literature:

3-amino-1,2,4-triazole; With hydrogenchloride; sodium nitrite;

1-Phenyl-4,4,4-trifluorobutane-1,3-dione; With sodium acetate; In ethanol; at 10 - 12 ℃;

DOI:10.1016/j.jfluchem.2005.06.001

Reference yield: 75.0%

6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine (886224-36-8) + methylhydrazine (60-34-4) → 3-(1-methyl-5-phenyl-3-trifluoromethylpyrazol-4-ylazo)-1H-1,2,4-triazole

Guidance literature:

In ethanol; for 8h; Heating;

DOI:10.1016/j.jfluchem.2005.06.001

Reference yield: 71.0%

6-benzoyl-7-hydroxy-7-trifluoromethyl-4,7-dihydro[1,2,4]triazolo[5,1-c][1,2,4]triazine (886224-36-8) + phenylhydrazine (100-63-0) → 3-(1,5-diphenyl-3-trifluoromethylpyrazol-4-ylazo)-1H-1,2,4-triazole

Guidance literature:

In ethanol; for 8h; Heating;

DOI:10.1016/j.jfluchem.2005.06.001

upstream raw materials:

1-Phenyl-4,4,4-trifluorobutane-1,3-dione

3-amino-1,2,4-triazole

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