1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

Base Information

Chemical Name:1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne
CAS No.:672958-79-1
Molecular Formula:C₂₃H₂₆FeOSi
Molecular Weight:402.391
Hs Code.:

Synonyms:1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

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Chemical Property of 1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

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Technology Process of 1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

There total 1 articles about 1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 292626-06-3
1-ferrocenyl-3-(trimethylsilyl)-1-phenylprop-2-yn-1-ol

: 74-88-4
methyl iodide

: 672958-79-1
1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

Guidance literature:: With methyllithium; In tetrahydrofuran; diethyl ether; an ethereal MeLi soln. was added at -60°C under Ar to a THF soln.of silylated propynol, the stirred soln. was allowed to warm to -25.deg ree.C, MeI was added, the mixt. was stirred overnight at room temp.; volatiles were removed in vacuo, residue was dissolved in ether, soln. washed with aq. NaHCO3 and water, dried over Na2SO4, evapd.; elem. anal.;

Reference yield: 84.2%

: 672958-79-1
1-ferrocenyl-1-methoxy-3-trimethylsilyl-1-phenylpropyne

: 672958-80-4
1-ferrocenyl-1-methoxy-1-phenylpropyne

Guidance literature:: With potassium hydroxide; In methanol; a suspn. of silylated ether and solid KOH in MeOH was stirred under Ar at room temp. for 12 h; evapd. in vacuo, residue was dissolved in ether, soln. washed with aq. NaHCO3 and water, dried over Na2SO4 and evapd.; elem. anal.;