allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

Base Information

Chemical Name:allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate
CAS No.:1051945-79-9
Molecular Formula:C₁₃H₁₄O₅
Molecular Weight:250.251
Hs Code.:

Synonyms:allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

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Chemical Property of allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

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Technology Process of allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

There total 1 articles about allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4136-21-4
p-methoxybenzoylmethanol

: 2937-50-0
Allyl chloroformate

: 1051945-79-9
allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/ja8038954

Reference yield: 56.0%

: 1051945-79-9
allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

: 3282-30-2
pivaloyl chloride

: 1051945-81-3
(Z)-2-(allyloxycarbonyloxy)-2-(4-methoxyphenyl)vinyl pivalate

Guidance literature:: allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1.08333h;

pivaloyl chloride; In tetrahydrofuran; at -78 - 23 ℃;
DOI:10.1021/ja8038954

Reference yield: 52.0%

: 1051945-79-9
allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate

: 75-36-5
acetyl chloride

: 1051945-80-2
(Z)-2-(allyloxycarbonyloxy)-2-(4-methoxyphenyl)vinyl acetate

Guidance literature:: allyl 2-(4-methoxyphenyl)-2-oxoethyl carbonate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1.05h;

acetyl chloride; In tetrahydrofuran; at -78 - 23 ℃; for 0.666667h;
DOI:10.1021/ja8038954