[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

Base Information

Chemical Name:[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate
CAS No.:1065267-43-7
Molecular Formula:C₄H₆O₆*C₁₅H₁₇FN₂
Molecular Weight:394.4
Hs Code.:

Synonyms:[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

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Chemical Property of [(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

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Technology Process of [(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

There total 5 articles about [(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-69-4,138508-61-9
L-Tartaric acid

: [1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine

: 1065267-43-7
[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

Guidance literature:: In ethanol; at 18 - 25 ℃;

Reference yield:

: 41404-58-4
2-bromo-5-fluoropyridine

: 1065267-43-7
[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; toluene / 1 h / 25 - 30 °C

1.2: 4 h / 5 - 10 °C

2.1: toluene-4-sulfonic acid / toluene / 5 h / Heating / reflux

3.1: sodium tetrahydroborate; cerium(III) chloride / methanol / 0.25 h / -45 °C

4.1: ethanol / 18 - 25 °C

With sodium tetrahydroborate; cerium(III) chloride; isopropylmagnesium chloride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; toluene;

Reference yield:

: 915720-54-6
1-(5-fluoropyridin-2-yl)ethan-1-one

: 1065267-43-7
[(1S)-1-(5-fluoropyridin-2-yl)ethyl][(1S)-1-phenylethyl]amine 2,3-dihydroxysuccinate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 5 h / Heating / reflux

2: sodium tetrahydroborate; cerium(III) chloride / methanol / 0.25 h / -45 °C

3: ethanol / 18 - 25 °C

With sodium tetrahydroborate; cerium(III) chloride; toluene-4-sulfonic acid; In methanol; ethanol; toluene;