N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

Base Information

Chemical Name:N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide
CAS No.:946076-41-1
Molecular Formula:C₁₉H₂₁ClF₃NO₆S₃
Molecular Weight:548.025
Hs Code.:

Synonyms:N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

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Chemical Property of N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

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Technology Process of N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

There total 2 articles about N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 946076-65-9
O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

: 75-36-5
acetyl chloride

: 946076-41-1
N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 830-42-2
N-allyl-4-chlorobenzenesulfonamide

: 946076-41-1
N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2: 49 percent / DMAP / CH₂Cl₂ / 2 h / 0 - 20 °C

With dmap; dilauryl peroxide; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2007.04.091