O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

Base Information

• Chemical Name: O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate
• CAS No.: 946076-65-9
• Molecular Formula: C₁₅H₁₇ClF₃NO₄S₃
• Molecular Weight: 463.95

Synonyms:O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

Chemical Property of O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

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Technology Process of O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate

There total 1 articles about O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

dithiocarbonic acid O-ethyl ester S-(2-oxo-3,3,3-trifluoropropyl) ester (879688-14-9) + N-allyl-4-chlorobenzenesulfonamide (830-42-2) → O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate (946076-65-9)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1016/j.tet.2007.04.091

Reference yield: 74.0%

O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate (946076-65-9) + N-methoxylamine hydrochloride (593-56-6) → O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-methoxyimino-5,5,5-trifluoropentyl] dithiocarbonate (946076-66-0)

Guidance literature:

With pyridine; In ethanol;

DOI:10.1016/j.tet.2007.04.091

Reference yield: 49.0%

O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-oxo-5,5,5-trifluoropentyl] dithiocarbonate (946076-65-9) + acetyl chloride (75-36-5) → N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide (946076-41-1)

Guidance literature:

With dmap; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.tet.2007.04.091

upstream raw materials:

dithiocarbonic acid O-ethyl ester S-(2-oxo-3,3,3-trifluoropropyl) ester

N-allyl-4-chlorobenzenesulfonamide

Downstream raw materials:

O-ethyl S-[1-(4-chlorobenzenesulfonylaminomethyl)-4-methoxyimino-5,5,5-trifluoropentyl] dithiocarbonate

N-acetyl-N-[5'-acetoxy-2'-ethoxythiocarbonylsulfanyl-6,6,6-trifluorohex-4-en-1-yl]-4-chlorobenzenesulfonamide

N-[2-(4-chlorophenyl)-6,6,6-trifluoro-5-methoxyiminohexyl]acetamide

C₁₂H₁₁NClF₃

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