1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

Base Information

Chemical Name:1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene
CAS No.:1332523-99-5
Molecular Formula:C₁₈H₂₁F₆NO₅
Molecular Weight:445.359
Hs Code.:

Synonyms:1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

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Chemical Property of 1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

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Technology Process of 1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

There total 27 articles about 1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-89-8
2,2,2-trifluoroethanol

: 1332523-84-8
phenyl (Z)-3-{3,4,5-trimethoxy-2-[2-(trifluoroacetylamino)ethyl]phenyl}prop-2-enyl carbonate

: 1332523-74-6
(S)-1-ethenyl-2-trifluoroacetyl-5,6,7-trimethoxy-1,2,3,4-tetrahydroisoquinoline

: 1332523-99-5
1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-O,O'-(3,3'-bis(naphthalen-1-ylmethyl)-5,5',6,6'-tetramethyl-1,1'-biphenyl-2,2'-diyl)-N,N-dimethylphosphoramidite; In dichloromethane; at 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.125

Reference yield:

: 75-89-8
2,2,2-trifluoroethanol

: 1332523-88-2
1-methylethenyl (Z)-3-{3,4,5-trimethoxy-2-[2-(trifluoroacetylamino)ethyl]phenyl}prop-2-enyl carbonate

: 1332523-74-6
(S)-1-ethenyl-2-trifluoroacetyl-5,6,7-trimethoxy-1,2,3,4-tetrahydroisoquinoline

: 1332523-99-5
1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-O,O'-(3,3'-bis(naphthalen-1-ylmethyl)-5,5',6,6'-tetramethyl-1,1'-biphenyl-2,2'-diyl)-N,N-dimethylphosphoramidite; In dichloromethane; at 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.125

Reference yield:

: 75-89-8
2,2,2-trifluoroethanol

: 1332523-84-8
phenyl (Z)-3-{3,4,5-trimethoxy-2-[2-(trifluoroacetylamino)ethyl]phenyl}prop-2-enyl carbonate

: 1332523-74-6
(S)-1-ethenyl-2-trifluoroacetyl-5,6,7-trimethoxy-1,2,3,4-tetrahydroisoquinoline

: 1332523-98-4
1-[(Z)-3-phenoxyprop-1-enyl]-2-[2-(trifluoroacetylamino)-ethyl]-2,3,4-trimethoxybenzene

: 1332523-99-5
1-[(Z)-3-(2,2,2-trifluoroethoxy)prop-1-enyl]-2-[2-(trifluoroacetylamino)ethyl]-2,3,4-trimethoxybenzene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-O,O'-(3,3'-bis(naphthalen-1-ylmethyl)-5,5',6,6'-tetramethyl-1,1'-biphenyl-2,2'-diyl)-N,N-dimethylphosphoramidite; In dichloromethane; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.125